Tvorba kokristalov organokovinskih spojin z jodom in jodovimi spojinami

Klemenc, Sabina (avtor), Perdih, Franc (mentor)

V okviru diplomskega dela sem pripravila različne kokristale z jodom in jodovimi spojinami. Kokristale sem pripravila iz organokovinskih spojin in jodom oz. jodovih spojin v različnih stehiometričnih razmerjih. Reakcije sem izvedla ob dodatku topila in segrevanju, nato sem pustila zmesi stati na sobni temperaturi teden dni, pokrito s parafilmom, da sem dobila kristale primerne velikosti za nadaljno obdelavo. S pomočjo rentgenske praškovne analize smo posneli difraktograme in jih primerjali s simuliranimi difraktogrami.

• Jezik: Slovenski jezik
• Ključne besede: kokristali, jod, jodove spojine, rentgenska praškovna analiza
• Vrsta gradiva: Diplomsko delo/naloga
• Tipologija: 2.11 - Diplomsko delo
• Organizacija: FKKT - Fakulteta za kemijo in kemijsko tehnologijo
• Leto izida: 2021
• PID: 20.500.12556/RUL-133218
• COBISS.SI-ID: 89661699
• Datum objave v RUL: 17.11.2021

KLEMENC, Sabina, 2021, Tvorba kokristalov organokovinskih spojin z jodom in jodovimi spojinami [na spletu]. Diplomsko delo. [Dostopano 26 april 2025]. Pridobljeno s: https://repozitorij.uni-lj.si/IzpisGradiva.php?lang=slv&id=133218

Sekundarni jezik

• Jezik: Angleški jezik
• Naslov: Co-crystal formation of organometallic compounds with iodine and iodine compounds

Izvleček

As part of my degree work, I prepared various cocrystals with iodine and iodine compounds. The starting materials were prepared from organometallic compounds and iodine or of iodine compounds in different stoichiometric ratios. The reactions were performed with the addition of solvent and under heating then the solutions stand on room temperature for one week, covered with parafilm, to obtain crystals of suitable size for further processing. Using X-ray powder analysis, diffractograms were recorded and compared with simulated diffractograms.

• Ključne besede: cocrystals, iodine, iodine compounds, X - ray powder analysis