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Determination of biogenic amines in fresh fish and processed fish products using IC-MS/MS
ID
Kočar, Drago
(
Avtor
),
ID
Köse, Sevim
(
Avtor
),
ID
Tufan, Bekir
(
Avtor
),
ID
Ščavničar, Andrej
(
Avtor
),
ID
Pompe, Matevž
(
Avtor
)
PDF - Predstavitvena datoteka,
prenos
(2,06 MB)
MD5: C4F10BA15098386254AD151DB1A9767D
URL - Izvorni URL, za dostop obiščite
https://www.mdpi.com/2304-8158/10/8/1746
Galerija slik
Izvleček
A new method was proposed for the determination of underivatized biogenic amines based on ion-exchange chromatography coupled with mass spectrometry detection. The method was applied to the analysis of 10 biogenic amines in fresh and processed fish products. The amines were extracted from muscle tissue with water without any additional derivative step or sample clean-up. Separation of biogenic amines was done by the IonPac (4 × 50 mm) column, applying a gradient eluent by mixing formic acid (2 mol L$^{−1}$) and Milli-Q water (formic acid concentration from 400 mM to 2 M). The results demonstrated a linear response in the range of 0.01 to 10 mg L$^{−1}$. The detection limits for the fish products ranged from 20 ng/g up to around 400 ng/g for histamine and putrescine, respectively. Spermidine and spermine showed significantly higher detection limits. This current method can be used for the determination of biogenic amines in both fresh and processed fish products for regulatory purposes and monitoring food-safety issues relating to these amines, particularly histamine. It is also a useful method for evaluation of other commercial analytical test kits and commonly used methods that are possibly affected by the food matrix due to processing or other drawbacks arising from the derivatization process.
Jezik:
Angleški jezik
Ključne besede:
biogenic amines
,
determination
,
fish products
,
histamine
,
ion chromatography
,
MS/MS
Vrsta gradiva:
Članek v reviji
Tipologija:
1.01 - Izvirni znanstveni članek
Organizacija:
FKKT - Fakulteta za kemijo in kemijsko tehnologijo
Status publikacije:
Objavljeno
Različica publikacije:
Objavljena publikacija
Leto izida:
2021
Št. strani:
14 str.
Številčenje:
Vol. 10, iss. 8, art. 1746
PID:
20.500.12556/RUL-136021
UDK:
543.544.14:543.51:664.95
ISSN pri članku:
2304-8158
DOI:
10.3390/foods10081746
COBISS.SI-ID:
73813507
Datum objave v RUL:
07.04.2022
Število ogledov:
28198
Število prenosov:
104
Metapodatki:
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Objavi na:
Gradivo je del revije
Naslov:
Foods
Skrajšan naslov:
Foods
Založnik:
MDPI
ISSN:
2304-8158
COBISS.SI-ID:
512252472
Licence
Licenca:
CC BY 4.0, Creative Commons Priznanje avtorstva 4.0 Mednarodna
Povezava:
http://creativecommons.org/licenses/by/4.0/deed.sl
Opis:
To je standardna licenca Creative Commons, ki daje uporabnikom največ možnosti za nadaljnjo uporabo dela, pri čemer morajo navesti avtorja.
Začetek licenciranja:
01.08.2021
Sekundarni jezik
Jezik:
Slovenski jezik
Ključne besede:
biogeni amini
,
določitev
,
ribji izdelki
,
histamin
,
ionska kromatografija
,
masna spektrometrija
Projekti
Financer:
TUBITAK - Türkiye Bilimsel ve Teknolojik Araştırma Kurumu
Financer:
ARRS - Agencija za raziskovalno dejavnost Republike Slovenije
Številka projekta:
BI-TUR 2008-2010-4
Financer:
ARRS - Agencija za raziskovalno dejavnost Republike Slovenije
Številka projekta:
P1-0153
Naslov:
Raziskave in razvoj analiznih metod in postopkov
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