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Sinteza in karakterizacija modificirane aluminijeve zlitine EN 7075 za selektivno lasersko taljenje : doktorska disertacija
ID Velikajne, Nejc (Author), ID Medved, Jože (Mentor) More about this mentor... This link opens in a new window, ID Paulin, Irena (Comentor)

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Abstract
Doktorska disertacija raziskuje sintezo in karakterizacijo modificirane aluminijeve zlitine EN AW 7075 za selektivno lasersko taljenje (SLM). Raziskava se osredotoča na optimizacijo procesnih parametrov in modifikacijo kemijske sestave za izboljšanje mikrostrukturne celovitosti in mehanskih lastnosti. Poudarek disertacije je na težavnosti procesiranja zaradi visokih ohlajevalnih hitrosti izrazitih temperaturnih gradientov ter širokega temperaturnega intervala strjevanja zlitine. Omenjene karakteristike se odražajo v razpokah in poroznosti na makrostrukturni ravni pri procesu selektivnega laserskega taljenja. Eksperimentalni del vključuje termodinamične izračune, analizo in karakterizacijo vhodnega prahu zlitine ter optimizacijo procesnih parametrov brez in z uporabo predgrevanja. Rezultati so pokazali, da predgrevanje podlage pri 100 °C in 200 °C ni bistveno vplivalo na odpravo napak, medtem ko je predgrevanje pri 400 °C spremenilo morfologijo razpok v vročem. Razpok je bilo manj, vendar so bile večje, notranje napetosti pa so se sproščale. Kljub temu sama metoda predgrevanja ni zadostovala za odpravo razpok v vročem. Naslednja faza raziskave in eksperimentalnega dela je vključevala modifikacijo zlitine z dodatkom silicija, kar je vplivalo na območje strjevanja in izboljšalo lastnosti zlitine med strjevanjem. Modificirana zlitina z večjo vsebnostjo silicija je pokazala izboljšano, udrobljeno mikrostrukturo in zmanjšano nagnjenost k razpokam. Eksperimentalni rezultati so potrdili, da modificirana zlitina omogoča boljše procesiranje s tehnologijo SLM, kar vodi do manj napak in posledično boljših mehanskih lastnosti. Po selektivnem laserskem procesiranju je sledila študija toplotne obdelave s pomočjo DSC meritev. Vzorce smo toplotno obdelovali po postopku T6. Po izvedeni toplotni obdelavi smo vzorce mehansko obdelali ter izvedli natezne preizkuse. Poleg tega smo izvedli obsežno mikrostrukturno analizo z uporabo vrstičnega elektronskega mikroskopa (SEM) in presevnega elektronskega mikroskopa (TEM). Eksperimentalni rezultati so pokazali, da modificirana zlitina izkazuje homogeno in drobnozrnato mikrostrukturo brez vidnih razpok ter z zmanjšano poroznostjo. Natezna trdnost modificirane zlitine po SLM izdelavi dosega vrednosti natezne trdnosti do 480 MPa. V nasprotju z nemodificirano zlitino, ki zaradi prisotnosti napak (razpok in poroznosti) ni dosegla meje tečenja, so se vzorci zlitine EN AW 7075 po izdelavi s SLM porušili pri 80 MPa. Po toplotni obdelavi T6 vrednosti natezne trdnosti padejo za 10 %. Trdota materiala pade iz 162,2 HV0,5 na 140,9 HV0,5.

Language:Slovenian
Keywords:Selektivno lasersko taljenje (SLM), aluminijeva zlitina EN AW 7075, modifikacija kemijske sestave, mikrostruktura, mehanske lastnosti, toplotna obdelava, mikrostrukturna analiza.
Work type:Doctoral dissertation
Typology:2.08 - Doctoral Dissertation
Organization:NTF - Faculty of Natural Sciences and Engineering
Place of publishing:Ljubljana
Publisher:N. Velikajne
Year:2026
Number of pages:XIX, 95 f.
PID:20.500.12556/RUL-189696 This link opens in a new window
UDC:669
COBISS.SI-ID:300951043 This link opens in a new window
Publication date in RUL:13.10.2026
Views:141
Downloads:65
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Secondary language

Language:English
Title:Synthesis and characterization of EN 7075 aluminium alloy for selective laser melting : Ph. D. Thesis
Abstract:
Selective Laser Melting (SLM) has emerged as a transformative manufacturing technology, enabling the production of complex and highly precise components. However, processing high-strength aluminum alloys such as EN AW 7075 remains challenging due to issues including hot cracking, porosity, and pronounced microstructural instability. This research addresses these challenges through SLM process parameter optimization and targeted modification of the alloy's chemical composition to improve its processability and mechanical performance. The experimental work included thermodynamic calculations using Thermo-Calc software to predict phase stability and solidification behavior, as well as detailed characterization of the feedstock powder. Process parameters including laser power, scanning speed, and preheating temperature—were systematically varied to evaluate their influence on microstructure and mechanical properties. Initial results showed that conventional SLM conditions lead to significant defects. While preheating at 100 °C and 200 °C had only a limited effect, preheating at 400 °C changed the morphology of hot cracks, resulting in wider and less branched cracks. The results indicate that residual stresses were partially relieved through crack formation; however, preheating alone was insufficient to prevent cracking. To further enhance processability, the alloy composition was modified by adding silicon. This modification altered the solidification range and improved solidification behavior, resulting in a refined, more homogeneous microstructure with a significantly reduced tendency for hot cracking. Advanced characterization techniques-including Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive Spectroscopy (EDS), and synchrotron X-ray diffraction-confirmed a fine-grained microstructure with reduced porosity and no visible cracks. Silicon addition also contributed to grain refinement and enhanced overall structural integrity. Following SLM processing, the material was subjected to heat treatment studies supported by Differential Scanning Calorimetry (DSC). Samples were heat-treated according to the T6 regime, then machined and tensile-tested. The modified alloy exhibited a homogeneous, fine-grained microstructure and significantly improved mechanical performance. The tensile strength of the as-built modified alloy reached up to 480 MPa. In contrast, the unmodified SLM EN AW 7075 alloy, due to defects such as cracks and porosity, did not reach the yield strength, with failure occurring at approximately 80 MPa. After T6 heat treatment, the tensile strength of the modified alloy decreased by approximately 10%, while the hardness decreased from 162.2 HV0.5 to 140.9 HV0,5.

Keywords:Selective Laser Melting (SLM), aluminium alloy EN AW 7075, chemical composition modification, microstructure, mechanical properties, heat treatment, microstructural analysis.

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