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Primerjava lastnosti in mikrostruktur intraoralnih in ekstraoralnih kompozitov : diplomsko delo
ID Lalović Smej, Zoja (Author), ID Brunčko, Mihael (Mentor) More about this mentor... This link opens in a new window, ID Forjanič, Miran (Comentor), ID Bohinc, Klemen (Reviewer)

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Abstract
Uvod: Kompozitni materiali so najpogosteje uporabljeni materiali za dentalne restavracije zaradi njihovih fizikalnih in kemijskih lastnosti, estetske vrednosti ter zadovoljive klinične učinkovitosti. Sestavljeni so iz organske smolne matice, anorganske utrjevalne faze in veznih sredstev. Dentalne kompozite delimo na direktne (intraoralne), ki se polimerizirajo neposredno v ustni votlini, in indirektne (ekstraoralne), ki se strjujejo v nadzorovanih laboratorijskih razmerah. Namen: Namen diplomskega dela je bil primerjati lastnosti in mikrostrukturo intraoralnih in ekstraoralnih kompozitnih materialov v zobni protetiki. Glavni cilji so bili okarakterizirati mikrostrukturo izbranih kompozitov, izmeriti njihovo gostoto ter določiti upogibno trdnost, modul elastičnosti in deformacijo pri maksimalni obremenitvi. Metode dela: V teoretičnem delu smo uporabili deskriptivno metodo dela s pregledom obstoječe literature. Za eksperimentalni del smo pripravili vzorce treh kompozitov v dimenzijah 4 × 4 × 20 mm: G-aenial Universal Flo (intraoralni), VITA Vionic Dent Disc multiColor in VITA VM LC (oba ekstraoralna). Mikrostrukturo smo analizirali s svetlobnim in vrstičnim elektronskim mikroskopom (SEM), mikrokemijsko sestavo smo določili z analizo EDS, gostoto smo izmerili s piknometrom, upogibne lastnosti pa smo določili z upogibnim preizkusom po standardu EN ISO 178:2003. Rezultati: Analiza SEM je pokazala, da ima G-aenial Universal Flo heterogeno dvofazno mikrostrukturo z lokalnimi mikroporoznostmi, VITA VM LC homogeno dvofazno mikrostrukturo, VITA Vionic Dent Disc multiColor pa trofazno zgradbo z dokaj enakomerno porazdelitvijo faz. Analiza EDS je potrdila prisotnost anorganskih polnil (SiO₂, Al, Sr) in organskih sestavin v vseh treh kompozitih. Najvišjo gostoto je dosegel G-aenial Universal Flo (1,7363 g/cm³), najnižjo pa VITA Vionic Dent Disc multiColor (1,2668 g/cm³). Upogibni preizkus je pokazal, da je najvišjo povprečno upogibno trdnost dosegel VITA VM LC (107,59 ± 5,41) MPa, sledil mu je G-aenial Universal Flo (102,65 ± 34,15) MPa, najnižjo pa VITA Vionic Dent Disc multiColor (74,42 ± 6,30) MPa. Najvišji modul elastičnosti je imel G-aenial Universal Flo (3268,20 ± 165,89) MPa. Razprava in zaključek: Raziskava je pokazala, da so mehanske lastnosti kompozitov neposredno odvisne od mikrostrukture, vrste polnil in kakovosti vezave med polimerno matico in utrjevalno fazo. VITA VM LC se je izkazal kot mehansko najbolj zanesljiv material s homogeno mikrostrukturo in najvišjo upogibno trdnostjo, primerljivo s podatki proizvajalca (≈ 110 MPa). G-aenial Universal Flo je kljub mikroporoznostim dosegel visoko togost, kar kaže na učinkovit polnilni sistem. VITA Vionic Dent Disc multiColor je primeren za estetsko usmerjene restavracije z nižjimi mehanskimi zahtevami. Rezultati potrjujejo, da izbira kompozita mora temeljiti na razumevanju mikrostrukture in namena uporabe.

Language:Slovenian
Keywords:diplomska dela, laboratorijska zobna protetika, dentalni kompoziti, mikrostruktura, mehanske lastnosti, upogibna trdnost, mikrokemijska analiza EDS
Work type:Bachelor thesis/paper
Typology:2.11 - Undergraduate Thesis
Organization:ZF - Faculty of Health Sciences
Place of publishing:Ljubljana
Publisher:[Z. Lalović Smej]
Year:2026
Number of pages:XII, 48 str., [7] str. pril.
PID:20.500.12556/RUL-184222 This link opens in a new window
UDC:616.31
COBISS.SI-ID:283323395 This link opens in a new window
Publication date in RUL:02.07.2026
Views:312
Downloads:148
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Secondary language

Language:English
Title:Comparison of properties and microstructures of intraoral and extraoral composites : diploma work
Abstract:
Introduction: Composite materials are the most used materials for dental restorations due to their physical and chemical properties, aesthetic value, and satisfactory clinical performance. They consist of an organic resin matrix, an inorganic reinforcing phase, and coupling agents. Dental composites are divided into direct (intraoral) composites, which polymerize inside the oral cavity, and indirect (extraoral) composites, which cure under controlled laboratory conditions, influencing their mechanical properties. Purpose: The aim of this study was to compare the mechanical properties and microstructure of intraoral and extraoral composite materials used in dental prosthetics. The main objectives were to characterize the microstructure of selected composites, measure their density, and determine flexural strength, elastic modulus, and strain at maximum load. Methods: The theoretical part was based on a review of existing literature using a descriptive method. For the experimental part, specimens of three composites (4 × 4 × 20 mm) were prepared: G-aenial Universal Flo (intraoral), VITA Vionic Dent Disc multiColor and VITA VM LC (both extraoral). Microstructure was analysed using light and scanning electron microscopy (SEM), chemical composition was determined by EDS analysis, density was measured using a pycnometer, and flexural properties were evaluated by a three-point bending test according to EN ISO 178:2003. Results: SEM analysis revealed a heterogeneous two-phase microstructure with local microporosity in G-aenial Universal Flo, a homogeneous two-phase microstructure in VITA VM LC, and a three-phase structure with fairly uniform phase distribution in VITA Vionic Dent Disc multiColor. EDS analysis confirmed the presence of inorganic fillers (SiO₂, Al, Sr) in all composites. The highest density was recorded for G-aenial Universal Flo (1.7363 g/cm³) and the lowest for VITA Vionic Dent Disc multiColor (1.2668 g/cm³). Flexural testing showed that VITA VM LC achieved the highest average flexural strength (107.59 ± 5.41) MPa, followed by G-aenial Universal Flo (102.65 ± 34.15) MPa, and VITA Vionic Dent Disc multiColor (74.42 ± 6.30) MPa. The highest elastic modulus was recorded for G-aenial Universal Flo (3268.20 ± 165.89) MPa. Discussion and conclusion: The study demonstrated that mechanical properties of composites are directly related to their microstructure, filler type, and quality of bonding between the polymer matrix and the reinforcing phase. VITA VM LC proved to be the most mechanically reliable material, with a homogeneous microstructure and flexural strength consistent with manufacturer specifications (≈ 110 MPa). G-aenial Universal Flo achieved high stiffness despite microporosity, indicating an efficient filler system. VITA Vionic Dent Disc multiColor is suitable for aesthetically oriented restorations with lower mechanical demands. The results confirm that composite selection should be based on understanding the microstructure and intended clinical application.

Keywords:diploma theses, laboratory dental prosthetics, dental composites, microstructure, mechanical properties, flexural strength, EDS microchemical analysis

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