Sinteza cinkovih in bakrovih kompleksov s heterocikličnimi karboksamidi

Kolbezen, Erik (author), Perdih, Franc (mentor)

V svojem diplomskem delu sem poizkusil sintetizirati cinkove(II) in bakrove(II) komplekse z osmimi še neraziskanimi heterocikličnimi amidi in vzgojiti kristale pridobljenih spojin. Kristali primerne kvalitete za rentgensko monokristalno analizo so nastali v dveh primerih, preostale vzorce sem analiziral z rentgensko praškovno difrakcijo. Z analizo sem ugotovil, da predvideni kompleksi niso nastali, v vzorcih so bile prisotne izhodne spojine.

• Language: Slovenian
• Keywords: cink(II), heterociklični karboksamidi, rentgenska praškovna difrakcija
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2025
• PID: 20.500.12556/RUL-172518
• COBISS.SI-ID: 255188739
• Publication date in RUL: 08.09.2025

Secondary language

• Language: English
• Title: Synthesis of zinc and copper complexes with heterocyclic carboxamides

Abstract

In my bachelor’s thesis I tried to synthesize zinc(II) and copper(II) complexes with eight yet unresearched heterocyclic amides and achieve crystal growth of obtained compounds. Crystals of required quality for single crystal X-ray diffraction formed in two instances, I analyzed the remaining samples with X-ray powder diffraction. Through the analysis I determined the predicted complexes did not form, the samples contained starting compounds.

• Keywords: zinc(II), heterocyclic carboxamides, X-ray powder diffraction