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Fluoridosilikati nekaterih piridinmetanolov
ID Jurinič, Tim (Author), ID Pevec, Andrej (Mentor) More about this mentor... This link opens in a new window

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Abstract
Temeljna podlaga dela je sinteza in karakterizacija koordinacijskih spojin, sintetiziranih iz nekaterih piridinmetanolov, natančneje iz 2-piridinmetanola, 3-piridinmetanola in 4-piridinmetanola s silicijevim dioksidom. Sinteze so potekale v raztopini fluorovodikove kisline, ki je bila reaktant in topilo hkrati. Reakcije so bile izvedene v dveh različnih množinskih razmerjih med piridinmetanolom in silicijevim dioksidom, ki sta bili 2 : 1 in 1 : 1. Iz raztopine se je s pomočjo počasnega izhlapevanja topila pri sobni temperaturi izločil trden produkt. Ta je bil nato karakteriziran z infrardečo spektroskopijo, $^1$H in $^{19}$F jedrsko magnetno resonančno spektroskopijo, elementno analizo ter rentgensko strukturno analizo.

Language:Slovenian
Keywords:piridinmetanol, fluorovodikova kislina, silicijev dioksid, infrardeča spektroskopija, rentgenska strukturna analiza
Work type:Bachelor thesis/paper
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Technology
Year:2025
PID:20.500.12556/RUL-171726 This link opens in a new window
COBISS.SI-ID:248757763 This link opens in a new window
Publication date in RUL:01.09.2025
Views:154
Downloads:47
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Secondary language

Language:English
Title:Fluoridosilicates of some pyridinemethanoles
Abstract:
The fundamental basis of the work is the synthesis and characterization of coordination compounds synthesized from some pyridinemethanols, more precisely from 2-pyridinemethanol, 3-pyridinemethanol and 4-pyridinemethanol with silicon dioxide. The syntheses were carried out in a solution of hydrofluoric acid, which was the reactant and solvent at the same time. The reactions were carried out in two different mass ratios between pyridinemethanol and silica, which were 2:1 and 1:1. A solid product was isolated from the solution by slow evaporation of the solvent at room temperature. The product was then characterized by infrared spectroscopy, $^1$H and $^{19}$F nuclear magnetic resonance spectroscopy, elemental analysis and X-ray structural analysis.

Keywords:pyridinemethanol, hydrofluoric acid, silicon dioxide, infrared spectroscopy, X-ray structural analysis

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