In the thesis, I present a project focused on the coating slurry preparation for catalyst coating in one segment of an automated production process. The goal was to develop a program for the Allen Bradley PLC, which controls the production process involving 36 fixed stations and 29 mobile tanks, pipes with valves and measurement sensors for fluid supply and mixers. Various process operations for preparing the coating slurry are performed within the combination of a fixed station and a mobile tank, after which the slurry is applied to ceramic or steel catalysts during the coating process. The basic suspensions, prepared in the tanks, consist of metal oxides, zeolites, acids, and bases, with the potential addition of platinum group metals or other catalytic metals. Continuous mixing of the suspension is necessary to prevent sedimentation of insoluble substances and solidification, which would result in tank damage. The addition of powdered substances is carried out manually, as material transfer monitoring and weighing are required for each batch preparation. Liquids are transferred from storage tanks to mobile tanks using pumps in an automated batch slurry preparation process.
The process is controlled by the Allen Bradley PLC, model 1756-L82E, with input-output signals connected to the 1734-AENTR module, commercially known as Point-IO. Since each tank operates as an independent unit, it has its own control cabinet with a cooling fan, containing the power module, fuses, Point-IO module, a frequency inverter for motor speed control using a potentiometer, safety relays with an emergency stop switch, and a network switch. The network switch connects the controller, frequency inverter, Point-IO module, and a scale for monitoring the amount of ingredients added to the tank. The program for the Allen-Bradley controller is written in the Studio 5000 development environment, and operators monitor the process through an HMI interface, which includes a SCADA system developed in Wonderware. The final product has resulted in lower production costs due to precise, faster, and more efficient system operation. The installed measuring devices provide the client with greater control over process data and final results. Enhanced safety for operators is also ensured, as they are not exposed to hazardous chemicals.
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