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Sinteza in karakterizacija nekaterih halopiridinijevih haksafluoridotitanatov
ID
Trogar, Kristina
(
Author
),
ID
Pevec, Andrej
(
Mentor
)
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Abstract
Pripravila in analizirala sem nekatere halopiridinijeve heksafluoridotitanatne soli. Za sintezo spojin sem uporabljala titanov dioksid, ki je nastal s hidrolizo titanovega(IV) butoksida. Tako pripravljen TiO2 pa je reagiral z ustreznim halopiridinom: 2-fluoropiridin, 2-kloropiridin, 2-bromopiridin in 3-bromopiridin. Reakcije med TiO2 in halopiridini sem izvedla v različnih množinskih razmerjih. Nastale produkte sem analizirala z infrardečo spektroskopijo, nuklearno magnetno resonančno spektroskopijo, elementno analizo in rentgensko strukturno analizo.
Language:
Slovenian
Keywords:
heksafluoridotitanat
,
halopiridin
,
vodikova vez
,
kristalna struktura
Work type:
Bachelor thesis/paper
Typology:
2.11 - Undergraduate Thesis
Organization:
FKKT - Faculty of Chemistry and Chemical Technology
Year:
2023
PID:
20.500.12556/RUL-151110
COBISS.SI-ID:
173434115
Publication date in RUL:
29.09.2023
Views:
1639
Downloads:
82
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TROGAR, Kristina, 2023,
Sinteza in karakterizacija nekaterih halopiridinijevih haksafluoridotitanatov
[online]. Bachelor’s thesis. [Accessed 7 July 2025]. Retrieved from: https://repozitorij.uni-lj.si/IzpisGradiva.php?lang=eng&id=151110
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Language:
English
Title:
Sinthesis and Characterization of some Halopyridinium Hexafluoridotitanates
Abstract:
Some halopyridinium hexafluoridotitanate salts have been prepared and characterised. Titanium dioxide, which was used for the synthesis of the compounds, was prepared by hydrolysis of titanium(IV) butoxide. The TiO2 thus prepared then reacted with corresponding halopyridine: 2-fluoropyridine, 2-chloropyridine, 2-bromopyridine and 3-bromopyridine. Reactions between TiO2 and halopyridine were carried out in different molar ratio. The resulting products were analysed by infrared spectroscopy, nuclear magnetic resonance spectroscopy, elemental analysis and X-ray structural analysis.
Keywords:
hexafluoridotitanate
,
halopyridine
,
hydrogen bond
,
crystal structure
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