Karakterizacija soli diatrizojične kisline

Črnič, Jaka (author), Perdih, Franc (mentor)

V diplomskem delu sem se ukvarjal z pripravo različnih soli oziroma kokristalov diatrizojične kisline tako, da sem poleg diatrizojične kisline uporabljal različna topila in številne reagente v različnih množinskih razmerjih in ugotavljal, katera razmerja so optimalna za pripravo produktov. Na koncu sem vzorce analiziral z rentgensko praškovno difrakcijo (PXRD) ter med seboj primerjal difraktograme.

• Language: Slovenian
• Keywords: diatrizojična kislina, kontrastna sredstva, halogenska vez, kokristali, rentgenska praškovna difrakcija
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2023
• PID: 20.500.12556/RUL-149320
• COBISS.SI-ID: 168113155
• Publication date in RUL: 06.09.2023

Secondary language

• Language: English
• Title: Characterization of diatrizoic acid salts

Abstract

In my bachelor’s thesis, I dealt with the preparation of various salts or co-crystals of diatrizoic acid by using, in addition to diatrizoic acid, various solvents and numerous reagents in different ratios and determining ratios are optimal for product formation. In the end, I analyzed the samples with X-ray powder diffraction (PXRD) and compared the diffractograms.

• Keywords: diatrizoic acid, contrast agents, halogen bond, co-crystals, X-ray powder diffraction