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Sinteza kelatnih analogov halicina
ID Krajnc, Tajda (Author), ID Kljun, Jakob (Mentor) More about this mentor... This link opens in a new window

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Abstract
Halicin je spojina, ki je sestavljena iz dveh heterocikličnih obročev, ki ju povezuje žveplov atom. V okviru diplomskega dela sem pripravila različne spojine podobne halicinu, v katerih sem spreminjala heterociklične substituente. Cilj raziskovalnega dela je bil optimizirati izkoristek reakcij in odstraniti prisotne nečistoče. Spojine sem karakterizirala z jedrsko magnetno resonanco, elementno analizo in masno spektrometrijo visoke ločljivosti. Kristali so bili karakterizirani z rentgensko strukturno analizo. Rezultati karakterizacij so pri nekaterih sintezah pokazali uspešno sintetiziran produkt.

Language:Slovenian
Keywords:halicin, sinteza, fizikalno-kemijska karakterizacija
Work type:Bachelor thesis/paper
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Technology
Year:2022
PID:20.500.12556/RUL-140001 This link opens in a new window
COBISS.SI-ID:128819203 This link opens in a new window
Publication date in RUL:09.09.2022
Views:583
Downloads:58
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Secondary language

Language:English
Title:Synthesis of chelating analogs of halicin
Abstract:
Halicin is a compound in which two heterocycles are connected by a sulfur atom. In the framework of the diploma thesis, I prepared different compounds similar to halicin in which I varied heterocyclic substituents. The goal of the research was to optimise the yield of reactions and to remove any impurities present. The compounds were characterized with nuclear magnetic resonance, elemental analysis and mass spectrometry of high resolution. The crystals were characterized by X-ray structural analysis. The results of characterizations have shown a successfully synthetised product in some syntheses.

Keywords:halicin, synthesis, physico-chemical characterization

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