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Analiza homogenizacije zlitine EN AW2011 z meritvijo električne prevodnosti
ID Einfalt, Lara (Author), ID Medved, Jože (Mentor) More about this mentor... This link opens in a new window

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Abstract
Čistemu aluminiju se z namenom izboljšanja mehanskih lastnosti dodajajo številni legirni elementi. Katerega od legirnih elementov bomo izbrali je odvisno od aplikacije oziroma uporabe zlitine. Za povečanje trdnosti in sposobnosti strojne obdelave dodajamo aluminiju baker. Ena izmed takšnih zlitin je zlitina EN AW2011, ki poleg 5.00–6.00 mas. % Cu vsebuje še svinec in bizmut. Ker poteka strjevanje zlitin v običajnih industrijskih praksah pri večjih hitrostih ohlajanja, nastajajo v mikrostrukturi nehomogenosti, izceje in intermetalne faze, ki se pri zlitinah serije 2xxx pojavljajo predvsem v obliki Al2Cu. S homogenizacijskim žarjenjem lahko zlitinam te serije zmanjšamo delež krhkih in neravnotežnih faz ter povprečno velikost faze Al2Cu, raztopimo topne komponente ter omogočimo bolj homogeno porazdelitev po mikrostrukturi. Cilj diplomskega dela je bil spremljanje homogenizacije aluminijeve zlitine EN AW2011 preko meritev specifične električne upornosti. V ta namen smo izdelali cilindrične vzorce in v vodoravni cevni uporovni električni peči opravili meritve specifične električne upornosti v odvisnosti od časa. Z namenom primerjalne analize smo 12 urno homogenizacijo izvajali pri dveh temperaturah, in sicer pri 480 in 520 °C ter izvedli DSC analizo. Po opravljenih meritvah smo izdelali krivulje poteka homogenizacije v odvisnosti od časa. Krivulje specifične električne upornosti so v prvih 100 minutah in DSC krivulje v prvih 50 minutah homogenizacijskega žarjenja na temperaturi 520 °C izrazito naraščale, medtem ko se je na krivuljah vzorcev, homogeniziranih pri 480 °C v prvih minutah žarjenja pred porastom pojavil še vrh oz. zastoj. V naslednjih urah homogenizacije se je naklon krivulj pri meritvah na obeh temperaturah uravnal. Zaključimo lahko, da se večina glavnih procesov homogenizacije EN AW2011 pri temperaturi 520 °C izvede v prvih 100 minutah homogenizacijskega žarjenja.

Language:Slovenian
Keywords:zlitina EN AW2011, homogenizacija, specifična električna upornost, DSC analiza
Work type:Bachelor thesis/paper
Organization:NTF - Faculty of Natural Sciences and Engineering
Year:2020
PID:20.500.12556/RUL-120758 This link opens in a new window
COBISS.SI-ID:33874691 This link opens in a new window
Publication date in RUL:25.09.2020
Views:955
Downloads:321
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Secondary language

Language:English
Title:Analysis of EN AW2011 alloy homogenization with electrical conductivity measurement
Abstract:
Numerous alloying elements are added to pure aluminum to improve its mechanical properties. Which of the alloying elements we choose depends on the application, the use of the alloy. Copper is added to aluminum to increase the strength and machinability. One of such alloys is the alloy EN AW2011, which in addition to 5.00 - 6.00 wt. % Cu also contains lead and bismuth. As the solidification of alloys in standard industrial practices occurs at higher cooling rates, inhomogeneities, leaks and intermetallic phases, mainly in the form of Al2Cu in alloys of the 2xxx series occur in the microstructure. By homogenization of this series's alloys, we can reduce the proportion of brittle and unbalanced phases and the average size of the Al2Cu phase, dissolve soluble components, and enable a more homogeneous distribution throughout the microstructure. The main aim of the diploma work was analysis of EN AW2011 alloy homogenization with electrical resistivity measurement. For this purpose, we made cylindrical samples and performed measurements of specific electrical resistance as a function of time in a horizontal tubular resistance electric furnace. For comparative analysis, 12-hour homogenization was conducted at two temperatures: 480 and 520 °C, and DSC analysis was performed. After the measurements, we made curves of the homogenization course as a function of time. The specific electrical resistivity curves increased markedly in the first 100 minutes and the DSC curves in the first 50 minutes of homogenization annealing at 520 °C, while on the curves of samples homogenized at 480 °C in the first minutes of annealing before rise there was an additional deviation. In the following hours of homogenization, the slope of the curves in the measurements at both temperatures was adjusted. It can be concluded that most of the main processes of EN AW2011 homogenization at a temperature of 520 °C are carried out in the first 100 minutes of homogenization annealing.

Keywords:alloy EN AW2011, homogenization, specific electrical resistivity, DSC analysis

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