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Adenin kot kation v heksafluoridosilikatnih soleh
ID
Brulc, Rok
(
Author
),
ID
Pevec, Andrej
(
Mentor
)
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Abstract
V diplomskem delu opisujem sintezo heksafluoridosilikatne soli s formulo [RH2]2+[SiF6]2- (1), v kateri je R adenin. Pri sintezi so bili kot reaktanti uporabljeni: SiO2, fluorovodikova kislina in adenin. Reakcija je bila izvedena v stehiometričnem razmerju 1 : 1 med SiO2 in adeninom, kar je vodilo do nastanka dvoprotoniranega adeninskega kationa. Iz raztopine fluorovodikove kisline so se izločili kristali, ki so bili nato analizirani z rentgensko strukturno analizo. Nastali produkt sem strukturno primerjal s spojino [RH]2+[SiF6]2- (R = adenin) (2) z že znano strukturo, ki vsebuje enoprotoniran adeninski kation.
Language:
Slovenian
Keywords:
Adenin
,
heksafluoridosilikati
,
rentgenska strukturna analiza
Work type:
Bachelor thesis/paper
Typology:
2.11 - Undergraduate Thesis
Organization:
FKKT - Faculty of Chemistry and Chemical Technology
Year:
2020
PID:
20.500.12556/RUL-119535
COBISS.SI-ID:
28379139
Publication date in RUL:
09.09.2020
Views:
2287
Downloads:
283
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BRULC, Rok, 2020,
Adenin kot kation v heksafluoridosilikatnih soleh
[online]. Bachelor’s thesis. [Accessed 26 July 2025]. Retrieved from: https://repozitorij.uni-lj.si/IzpisGradiva.php?lang=eng&id=119535
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Language:
English
Title:
Adenine as cation in hexafluoridosilicate
Abstract:
In this thesis I describe the synthesis of hexafluoridosilicate salt with formula [RH2]2+[SiF6]2-(1), where R is adenine. SiO2, hydrofluoric acid and adenine were used as reactants in the synthesis. The reaction was performed in a stoichiometric ratio of 1 : 1 between SiO2 and adenine, which led to the formation of a double-protonated adenine cation. Crystals were formed in hydrofluoric acid solution, which were then analyzed by X–ray crystallography. The structure of resulting product was compared with compound [RH]2+[SiF6]2- (R = adenine) (2) with known structure containing a monoprotonated adenine cation.
Keywords:
Adenine
,
hexafluoridosilicates
,
X-ray crystallography
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