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Vpliv staranja na trdoto volframa in volframovega kompozita s karbidnimi vključki
ID Simonič, David (Author), ID Petriček, Saša (Mentor) More about this mentor... This link opens in a new window

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Abstract
Eden od problemov načrtovanja fuzijske elektrarne je izbira materialov, ki bodo zdržali ekstremne pogoje bližine plazme. Primeren material bi bili lahko volframovi kompoziti. V čistem volframu pri visokih temperaturah poteka proces rekristalizacije, ki jo spremlja rast zrn, kar vodi do poslabšanja mehanskih lastnosti materiala. Potencialna rešitev je kompozit volframa z delci divolframovega karbida (W2C), ki omejijo rast volframovih zrn in s tem zavrejo rekristalizacijo. Pri diplomskem delu sem pripravil štiri zmesi prahov volframa in volframovega karbida (WC) različnih koncentracij. Vzorce sem zgostil s pomočjo tehnike SPS. Z SEM smo analizirali mikrostrukturo in z XRD fazno sestavo vzorcev. Trdoto pripravljenih vzorcev sem primerjal s trdoto istih vzorcev, ki so bili starani. Trdota kompozitov z večjim deležem W2C je višja. Trdota vzorcev pred staranjem in po staranju pri vseh temperaturah je enaka, zato sklepamo, da rekristalizacija med staranjem pri izbranih pogojih ni potekla.

Language:Slovenian
Keywords:volfram, volframov karbid, kompozit, rekristalizacija, staranje, trdota
Work type:Bachelor thesis/paper
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Technology
Year:2019
PID:20.500.12556/RUL-109950 This link opens in a new window
COBISS.SI-ID:1538422467 This link opens in a new window
Publication date in RUL:10.09.2019
Views:1072
Downloads:227
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Secondary language

Language:English
Title:Influence of ageing on hardness of tungsten and tungsten composites with tungsten carbide
Abstract:
One of the problems with designing fusion power plant is the choice of materials that will withstand extreme conditions in proximity of plasma. Suitable materials for this application could be tungsten composites. Pure tungsten starts to recrystallize at high temperatures, where grain growth occurs, and that leads to a deterioration of the mechanical properties of the material. A potential solution is a tungsten composite with ditungsten carbide (W2C) particles that limit the growth of tungsten grains and thus inhibit recrystallization. In my thesis I prepared four mixtures of tungsten and tungsten carbide (WC) powders of different concentrations. The samples were densified using the SPS technique. Microstructure was analyzed using SEM and the phase composition of the samples was determined using XRD. Hardness of the prepared samples was compared with the hardness of the same samples that were aged. The hardness of composites with higher W2C content is higher. The hardness of the specimens before and after aging at all temperatures is the same, so we can conclude that recrystallization in our samples did not occur under the selected conditions during aging.

Keywords:tungsten, tungsten carbide, composite, recrystallization, aging, hardness

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