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Idealni povečevalni efekt mikroreaktorja
ID Kreuh, Izak (Author), ID Plazl, Igor (Mentor) More about this mentor... This link opens in a new window

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Abstract
Mikroreaktorji nudijo izboljšan prenos toplote in snovi, večjo varnost in bolj zelen pristop za pridobivanje številnih kemijskih produktov. Poleg tega nudijo lažje obratovanje in zahtevajo manj stroškov, povezanih s tem. V njih lahko dosežemo različne tokovne pogoje in izdelani so lahko iz raznolikih materialov. Za večje proizvode se jih pogosto uporabi več v seriji ali pa se izvede povečevalni efekt, katerega učinkovitost se preveri s pomočjo dimenzijske analize ali s pomočjo modela. V tej magistrski nalogi sem uporabil mrežno Boltzmannovo metodo z globinskim povprečenjem, da sem pripravil psevdodvodimenzionalen model mikroreaktorja realnih dimenzij z zapleteno vstopno geometrijo. Rezultate modela sem preveril v laboratoriju, kjer sem spremljal redčenje sledilca (vodne raztopine rdečega barvila za živila) po mikrokanalu. Ugotovil sem, da model zanesljivo oblikuje primerljive tokovne profile, vendar pa je pri samih vrednostih hitrosti prišlo do večjega odstopanja. Sklepal sem, da so za večje odstopanje krivi predvsem moj pristop merjenja v laboratoriju in težave pri analizi pridobljenega videa. Za bodočo laboratorijsko preverjanje modelov povečevalnega efekta mikroreaktorjev bi predlagal uporabo boljše snemalne opreme, sledilca temnejše barve, barve z večjim kontrastom, uporabo fluorescentnega sledilca ali pa merjenje hitrosti z mikrodelci.

Language:Slovenian
Keywords:mikroreaktor, mrežna Boltzmannova metoda, povečevalni efekt, globinsko povprečenje
Work type:Master's thesis/paper
Typology:2.09 - Master's Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Technology
Year:2024
PID:20.500.12556/RUL-161754 This link opens in a new window
COBISS.SI-ID:215977475 This link opens in a new window
Publication date in RUL:13.09.2024
Views:138
Downloads:26
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Secondary language

Language:English
Title:Ideal scale-up of microreactor
Abstract:
Microreactors produce better transport phenomena, have better safety outcomes and are a greener solution for producing a wide range of chemical compounds. They are also easier and cheaper to manage. They can accommodate a wide range of flow patterns and can be made from a large pool of materials. Numbering-up is a common way to increase their output as well as scaling-up. The effectiveness of scaling-up can be determined by a dimensional analysis or by using a model. In this work I used a lattice Boltzmann model with a depth-averaged approach to model the flow of a microreactor of real dimension. I then compared the model results with the results obtained in a lab setting by a dilution-based characterisation method, in which I measured the flow speed by sending a tracer solution (red food dye diluted in water) through the microchannel. I discovered that the model can reliably predict the flow profile, but the actual values of the flow velocity do differ by a noticeable amount. I concluded that the difference in the value of flow velocity is mainly due to my measuring approach and difficulty in analysing the resulting video. For further experimentation I suggest using better recording equipment, a darker, more contrasting or even a fluorescent tracer or perhaps by using micro image velocimetry.

Keywords:microreactor, lattice Boltzmann method, scale-up, depth-averaged approach

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