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Karakterizacija toplotno obdelane nikljeve superzlitine Inconel 718 izdelane s selektivnim laserskim taljenjem : magistrsko delo
ID Krek, Gašper (Author), ID Nagode, Aleš (Mentor) More about this mentor... This link opens in a new window, ID Malej, Simon (Comentor)

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Abstract
Superzlitine so skupina zlitin, ki izkazujejo odlične mehanske lastnosti in korozijsko odpornost tudi pri povišanih temperaturah. Mednje sodi tudi nikljeva superzlitina Inconel 718. Komponente iz Inconela 718 je mogoče izdelati tudi s procesom selektivnega laserskega taljenja, po procesu pa je potrebno izvesti še toplotno obdelavo, saj se med strjevanjem izločajo neželene faze, ki lahko vplivajo na mehanske lastnosti materiala. V magistrskem delu smo preučili vpliv temperature in časa raztopnega žarjenja na razvoj mikrostrukture in izločanje faz med toplotno obdelavo na temperaturnem intervalu od 1000 do 1200 °C, po časih žarjenja 10, 20, 30, 60 in 120 minut. S pomočjo EBSD analize smo določili velikost kristalnih zrn, delež rekristalizacije, teksturo in delež dvojčičnih mej v mikrostrukturi. Ugotovili smo, da se je rekristalizacija pričela pri 1050 °C med časoma 10 in 20 minut. Pri višjih temperaturah se je pričela med 0 in 10 minutami žarjenja, rast kristalnih zrn pa je potekala hitro. Preučili smo tudi vpliv temperature žarjenja na mehanske lastnosti materiala pri sobni temperaturi. Primerjali smo lastnosti po žarjenju na 954, 1000 in 1100 °C, v prečni smeri in vzdolžno na smer gradnje, da smo določili anizotropijo mehanskih lastnosti. Z žarjenjem na 1000 °C smo izboljšali napetost tečenja in znižali duktilnost, medtem ko smo z žarjenjem na 1100 °C znižali trdnostne lastnosti, vendar izboljšali duktilnost. Anizotropija po žarjenju na 1000 °C je ostala, po žarjenju na 1100 °C pa se je smerna odvisnost trdnostnih lastnosti zmanjšala.

Language:Slovenian
Keywords:selektivno lasersko taljenje, Inconel 718, toplotna obdelava, mikrostrukturna analiza, anizotropija
Work type:Master's thesis/paper
Typology:2.09 - Master's Thesis
Organization:NTF - Faculty of Natural Sciences and Engineering
Place of publishing:Ljubljana
Publisher:G. Krek
Year:2024
Number of pages:XVI, 77 f.
PID:20.500.12556/RUL-161724 This link opens in a new window
UDC:669
COBISS.SI-ID:211939331 This link opens in a new window
Publication date in RUL:13.09.2024
Views:194
Downloads:54
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Secondary language

Language:English
Title:Characterization of heat-treated nickel-based superalloy Inconel 718 manufactured by laser powder bed fusion : master's thesis
Abstract:
Superalloys are a group of alloys that exhibit excellent mechanical properties and corrosion resistance even at elevated temperatures. Among them is the nickel-based superalloy Inconel 718. Components made from Inconel 718 can also be produced by the selective laser melting process; however, heat treatment is required after the process, as undesirable phases that can affect the material's mechanical properties precipitate during solidification. In this master's thesis, the influence of solution annealing temperature and time on the microstructure development and phase precipitation during heat treatment was investigated in the temperature range of 1000 to 1200 °C, with annealing times of 10, 20, 30, 60, and 120 minutes. EBSD analysis was used to determine crystal grain size, recrystallization fraction, texture, and the fraction of twin boundaries in the microstructure. It was found that recrystallization began at 1050 °C between 10 and 20 minutes. At higher temperatures, recrystallization started between 0 and 10 minutes of annealing, and grain growth proceeded rapidly. The influence of annealing temperature on the mechanical properties of the material at room temperature was also studied. Properties were compared after annealing at 954, 1000, and 1100 °C, transversely and longitudinally to the build direction, to determine the anisotropy of mechanical properties. After annealing at 1000 °C, the yield strength was improved and ductility was reduced, while annealing at 1100 °C decreased the strength properties but improved ductility. Anisotropy remained after annealing at 1000 °C, whereas after annealing at 1100 °C, the directional dependence of strength properties was reduced.

Keywords:laser powder bed fusion, Inconel 718, heat treatment, microstructure analysis, anisotropy

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