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Izolacija nanoceluloze iz juvenilne in adultne smrekovine : diplomski projekt
ID Pongrac, Matjaž (Author), ID Poljanšek, Ida (Mentor) More about this mentor... This link opens in a new window, ID Vek, Viljem (Comentor), ID Oven, Primož (Reviewer)

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Abstract
Cilj diplomske naloge je bila priprava nanoceluloze iz juvenilnega in adultnega lesa smrekovine. Predelava materiala je potekala od kolutov lesa, do zelo majhnih nano delcev. Z razrezom in mletjem smo les najprej dezintegrirali do lesnega prahu, nato pa ga s kemičnimi postopki čiščenja, delignifikacije in odstranjevanja hemiceluloz obdelovali dokler nismo dobili [alfa]-celuloze. Tem postopkom je sledila TEMPO oksidacija in mehanska obdelava. Na ta način smo uspeli pridobiti suspenzijo, ki je vsebovala celulozna vlakna, fragmente celuloznih vlaken in fragmente njihovih celičnih sten ter zelo majhne delce, ki so formirali gel. Ta je izkazoval značilnosti gela, ki je sicer značilen za nanofibrilirano celulozo. Postopek je mogoče bistveno izboljšati z izborom vhodnega materiala, finejšim mletjem ter učinkovitejšo kemično in mehansko obdelavo materiala.

Language:Slovenian
Keywords:smreka, celuloza, nanoceluloza, TEMPO oksidacija
Work type:Diploma project paper
Typology:2.11 - Undergraduate Thesis
Organization:BF - Biotechnical Faculty
Place of publishing:Ljubljana
Publisher:M. Pongrac
Year:2016
Number of pages:VII, 29 f.
PID:20.500.12556/RUL-158781 This link opens in a new window
UDC:630*813
COBISS.SI-ID:2637193 This link opens in a new window
Publication date in RUL:20.06.2024
Views:199
Downloads:10
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Secondary language

Language:English
Title:Isolation of nanocelulose from juvenile and adult wood of Norway spruce : B. Sc. thesis
Abstract:
The goal of this research was the isolation of nanocellulose from juvenile and adult wood of Norway spruce. The process was done first by mechanically sewing and grinding the wood to make wood dust. The next step was the chemical treatment by organic solvents in order to remove polar and non-polar extractives from the wood dust. Next two steps were delignification and the removal of hemicellulose, the result of which was [alpha]-cellulose. Then we used TEMPO oxidation and mechanical processing for the disintegration of the cellulose fibers. Next two steps were TEMPO oxidation and mechanical treatment. This way we were able to acquire a substance that contained cellulose fibers, fragments of cellulose fibers, fragments of cell walls and small particles that formed a gel. This gel was similar to the type of gel that is characteristic to the one formed by nanocellulose. The process that was used can be drastically improved by a better selection of input material, finer grinding and more effective chemical and mechanical treatment.

Keywords:Norway spruce, cellulose, nanocellulose, TEMPO oxidation

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