Sinteza in karakterizacija koordinacijskih spojin s fenilocetno kislino

Rajk, Žan (author), Kozlevčar, Bojan (mentor)

Sintetiziral in opisal sem dve modri bakrovi(II) in eno belo cinkovo(II) koordinacijsko spojino s fenilocetno kislino (= HL = C8H8O2). Dobljene spojine imajo formulo: [Cu(L)2]n, Cu(L)2(nia)2 (nia = nikotinamid = C6H6N2O) in [Zn(L)2]n. Kot topilo sem uporabil vodo ali metanol. Uporabljal sem tudi dodatni nevtralni ligand nikotinamid. Končne vzorce sem analiziral s praškovno rentgensko difrakcijo, IR spektroskopijo, ter z UV-Vis spektroskopijo.

• Language: Slovenian
• Keywords: baker(II), cink(II), fenilocetna kislina, nikotinamid, koordinacijske spojine, struktura
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2022
• PID: 20.500.12556/RUL-139051
• COBISS.SI-ID: 121680131
• Publication date in RUL: 29.08.2022

Secondary language

• Language: English
• Title: Synthesis and characterization of coordination compounds with phenylacetic acid

Abstract

Two copper(II) and one zinc(II) coordination compound with phenylacetic acid (= HL = C8H8O2) were synthesized. The formulas of obtained compounds are : [Cu(L)2]n, Cu(L)2(nia)2 z (nia = nicotinamide = C6H6N2O) and [Zn(L)2]n. I used water or methanol as solvent. I also used an additional neutral ligand, nicotinamide. The final samples were analysed by X-ray powder diffraction, IR spectroscopy and UV-Vis spectroscopy.

• Keywords: copper(II), zinc(II), phenylacetic acid, nicotinamide, coordination compounds, structure