Luminiscenčne lastnosti cinkovih koordinacijskih spojin z diketonatnimi in karboksilatnimi ligandi

Bradeško, Hanno (author), Perdih, Franc (mentor)

V okviru diplomskega dela sem spremljal luminiscenco vzorcev cinkovih koordinacijskih spojin. Pri snemanju UV-Vis spektrov sem uporabljal nastavljeno valovno dolžino od 800 do 200 nm in sicer na prestopnem intervalu 2 nm. Z merjenjem fluorescence prvega slepega vzorca sem ugotovil najboljše meritve za odprtino reže pri 15-15 nm, 10-15 nm in 5-15 nm. Na podlagi teh slepih vzorcev sem nato meril svoje vzorce na fluorimetru. Čistost vzorcev sem preveril tudi z 1H jedrsko magnetno spektroskopijo.

• Language: Slovenian
• Keywords: luminiscenca, fluorescenca, vzorec
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2020
• PID: 20.500.12556/RUL-117461
• COBISS.SI-ID: 23482115
• Publication date in RUL: 10.07.2020

Secondary language

• Language: English
• Title: Luminescene properties of zinc coordination compounds with diketonato and carboxylato ligands

Abstract

In my diploma thesis, I have measured luminescence of two samples of zinc coordination compounds. For a measurement of UV-VIS spectrum, wavelength from 800 to 200 nm on an interval of 2 nm was used. By measuring a fluorescence of a blind sample, I discovered the best three measurements for open slit were at 15-15 nm, 10-15 nm and 5-15 nm. According on these results obtained by blind samples, I continued to measure my samples on fluorimeter. I also checked the purity of the samples by 1H nuclear magnetic resonance spectroscopy.

• Keywords: uminescence, fluorescence, sample