Kompleks železovega(III) klorida s piridin-2-onom

Krivic, Erika (author), Petriček, Saša (mentor)

Po reakciji med FeCl3·6H2O in pridin-2-onom v etanolu pri sobni temperaturi nastane suspenzija, ki smo jo filtrirali. Iz filtrata kristalizira spojina [Fe(C5H5NO)6]·[FeCl4]2·Cl. Enaka je tudi struktura nastale oborine. Sestavo in strukturo smo potrdili s CHN analizo, infrardečo spektroskopijo, rentgensko praškovno in rentgensko strukturno analizo.

• Language: Slovenian
• Keywords: železov(III) klorid, piridin-2-on, kristalizacija, kompleks
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2019
• PID: 20.500.12556/RUL-113517
• COBISS.SI-ID: 1538301379
• Publication date in RUL: 15.01.2020

Secondary language

• Language: English
• Title: Iron(III) chloride complex with pyridine-2-one

Abstract

A reaction of FeCl3·6H2O and the pyridin-2-one in ethanol at room temperature resulted in a suspension, which was filtered. From the filtrate crystallized the compound [Fe(C5H5NO)6]·[FeCl4]2·Cl. The content and structure of the crystals and precipitate were confirmed by CHN analysis, infrared spectroscopy, X-ray powder analysis and single crystal X-ray analysis.

• Keywords: iron(III) chloride, pyridin-2-one, crystallization, complex