Pretvorbe ketonov pri pogojih brez topila

Abdić, Edisa (author), Jereb, Marjan (mentor)

Tekom diplomske naloge sem izvajala reakcije pod pogoji brez topila. Iz različnih ketonov in fenilacetilena sem v prisotnosti kalijevega terc-butoksida s trenjem v terilnici sintetizirala propargilne alkohole z dobrimi izkoristki pri sobni temperaturi. Produkte sem izolirala z ekstrakcijo in destilacijo topila ter nato izvedla še analizo z 1H NMR spektroskopijo. Spektri so bili posneti v CDCl3 pri 300 MHz.

• Language: Slovenian
• Keywords: Ketoni, zelena kemija, propargilni alkoholi
• Work type: Bachelor thesis/paper
• Typology: 2.11 - Undergraduate Thesis
• Organization: FKKT - Faculty of Chemistry and Chemical Technology
• Year: 2019
• PID: 20.500.12556/RUL-110790
• COBISS.SI-ID: 1538436035
• Publication date in RUL: 19.09.2019

Secondary language

• Language: English
• Title: Transformation of ketones under solvent-free conditions

Abstract

During the Diploma work I carried out reactions under solvent free conditions. From different ketones and phenylacetylene and in the presence of potassium tert-butoxide, I synthesized propargyl alcohols with good yields and at room temperature, with grinding in the mortar. I isolated the products with extraction and solvent distillation. Then I analyzed the products with 1H NMR spectroscopy. Spectra were recorded in CDCl3 at 300 MHz.

• Keywords: Ketones, green chemistry, propargyl alcohol