The purpose of my thesis was to prepare and characterize iron and copper coordination compounds of thiohydroxamic acids. Two thiohydroxamic acids were prepared and their synthesis protocols were optimized. Complexes of said acids and complexes with three other acids were prepared. The synthesized acids were characterized with nuclear magnetic resonance (NMR), mass spectrometry and IR spectroscopy. Prepared coordination compounds were characterized with mass spectrometry, elemental analysis CHN, IR and UV-Vis spectroscopy.
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