20.500.12556/RUL-187761 Fluoridotitanati nekaterih hidroksimetilpiridinov Fluoridotitanates of some hydroxymethylpyridines V diplomski nalogi opisujem sintezo in karakterizacijo treh novih spojin 1-3, ki so bile sintetizirane iz 2-(hidroksimetil)piridina, 3-(hidroksimetil)piridina in 4-(hidroksimetil)piridina ter titanovega(IV) butoksida. Titanov(IV) butoksid sem raztopila v vodi, da je nastal trden titanov dioksid. Fluorovodikova kislina je bila uporabljena kot reaktant in topilo. Reakcije so bile izvedene med ustreznim hidroksimetilpiridinom in titanovim dioksidom v množinskem razmerju 2 : 1. Vsak produkt, ki se je izločil po izhlapevanju topila pri sobni temperaturi, je bil v kristalinični obliki. Produkte sem karakterizirala z elementno (CHN) analizo, IR spektroskopijo, NMR spektroskopijo in rentgensko strukturno analizo ter določila izkoristek sinteze. Described are the synthesis and characterization of three novel compounds 1-3, which are prepared from 2-(hydroxymethyl)pyridine, 3-(hydroxymethyl)pyridine, 4-(hydroxymethyl)pyridine and titanium(IV) butoxide. Titanium(IV) butoxide is dissolved in water to form a solid titanium dioxide. Hydrofluoric acid was used as the reactant as well as the solvent. The reactions were carried out between corresponding hydroxymethylpyridine and titanium dioxide in a molar ratio of 2:1. Each product precipitated after evaporation of the solvent at room temperature was in crystalline form. The products were characterized by elemental (CHN) analysis, IR spectroscopy, NMR spectroscopy and X-ray structural analysis along with the yield of the synthesis determination. fluoridotitanati hidroksimetilpiridin sinteza struktura fluoridotitanates hydroxymethylpyridine synthesis structure true false false Slovenski jezik Angleški jezik Diplomsko delo/naloga 2026-09-14 07:20:06 2026-09-14 07:20:15 2026-09-16 03:42:39 0000-00-00 00:00:00 2026 0 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 1970-01-01 25646 Bobnar_Zala_-_Fluoridotitanati_nekaterih_hidroksimetilpiridinov.pdf Bobnar_Zala_-_Fluoridotitanati_nekaterih_hidroksimetilpiridinov.pdf 1 2C868FBAFCF7C1ABCE6600B97D051063 d5c258959c52633a587f9a90da0d2105a03baee5e0eeadb84db3e1886ba72602 f32a011b-affb-11f1-8bc5-0050569b8976 https://repozitorij.uni-lj.si/Dokument.php?lang=slv&id=247503 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0