20.500.12556/RUL-162985 PIRIDINPROPANOL KOT KATION V NEKATERIH FLUORIDOMETALATNIH SOLEH PYRIDINEPROPANOL AS CATION IN SOME FLUORIDOMETALATE SALTS Izvedel sem reakcije s tremi različnimi piridinpropanoli kot so: 2-piridinpropanol, 3-piridinpropanol in 4-piridinpropanol, z nekaterimi oksidi in sicer s silicijevim dioksidom, titanovim dioksidom in vanadijevim(V) oksidom. Reakcije sem izvajal v fluorovodikovi kislini v množinskih razmerjih med kovinskim oksidom in ustreznim piridinpropanolom 1:1 in 2:1. Po reakciji je potekala kristalizacija s pomočjo odhlapevanja topila, fluorovodikove kisline. Nastale kristale sem analiziral z infrardečo spektroskopijo, nuklearno magnetno resonančno spektroskopijo in rentgensko strukturno analizo. Trem novim spojinam je bila določena kristalna struktura. I performed reactions between three different pyridinepropanols such as: 2-pyridinepropanol, 3-pyridinepropanol and 4-pyridinepropanol, with some oxides namely silicon dioxide, titanium dioxide and vanadium(V) oxide. Reactions took place in hydrofluoric acid in molar ratio 1:1 and 1:2 between metallic oxide and corresponding pyridinepropanol. After the reaction the mixture was left for crystallisation in fume hood. Crystallised products were analysed with infrared spectroscopy, nuclear magnetic resonance spectroscopy and X-ray structural analysis. Three new crystal structures were obtained. koordinacijske spojine fluoridometalati piridinpropanol rentgenska strukturna analiza infrardeča spektroskopija coordination compounds fluorometalates pyridinepropanol X-ray structural analysis infrared spectroscopy true false false Slovenski jezik Angleški jezik Diplomsko delo/naloga 2024-09-30 10:20:01 2024-09-30 10:20:06 2024-12-05 10:25:12 0000-00-00 00:00:00 2024 0 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 23092 217779971 Vincec_Nejc_-_PIRIDINPROPANOL_KOT_KATION_V_NEKATERIH_FLUORIDOMETALATNIH_SOLEH.pdf Vincec_Nejc_-_PIRIDINPROPANOL_KOT_KATION_V_NEKATERIH_FLUORIDOMETALATNIH_SOLEH.pdf 1 2BDD34BDD3E083370286176B16037932 55f1635a56cdbca654a04a0331bf75a34709e0ebd0c443110cc7c585732e8510 a79df0b6-7f04-11ef-b232-0050569b8976 https://repozitorij.uni-lj.si/Dokument.php?lang=slv&id=192434 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0