20.500.12556/RUL-151110 Sinteza in karakterizacija nekaterih halopiridinijevih haksafluoridotitanatov Sinthesis and Characterization of some Halopyridinium Hexafluoridotitanates Pripravila in analizirala sem nekatere halopiridinijeve heksafluoridotitanatne soli. Za sintezo spojin sem uporabljala titanov dioksid, ki je nastal s hidrolizo titanovega(IV) butoksida. Tako pripravljen TiO2 pa je reagiral z ustreznim halopiridinom: 2-fluoropiridin, 2-kloropiridin, 2-bromopiridin in 3-bromopiridin. Reakcije med TiO2 in halopiridini sem izvedla v različnih množinskih razmerjih. Nastale produkte sem analizirala z infrardečo spektroskopijo, nuklearno magnetno resonančno spektroskopijo, elementno analizo in rentgensko strukturno analizo. Some halopyridinium hexafluoridotitanate salts have been prepared and characterised. Titanium dioxide, which was used for the synthesis of the compounds, was prepared by hydrolysis of titanium(IV) butoxide. The TiO2 thus prepared then reacted with corresponding halopyridine: 2-fluoropyridine, 2-chloropyridine, 2-bromopyridine and 3-bromopyridine. Reactions between TiO2 and halopyridine were carried out in different molar ratio. The resulting products were analysed by infrared spectroscopy, nuclear magnetic resonance spectroscopy, elemental analysis and X-ray structural analysis. heksafluoridotitanat halopiridin vodikova vez kristalna struktura hexafluoridotitanate halopyridine hydrogen bond crystal structure true false false Slovenski jezik Angleški jezik Diplomsko delo/naloga 2023-09-29 14:15:00 2023-09-29 14:15:03 2023-11-23 12:58:08 0000-00-00 00:00:00 2023 0 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 23014 173434115 Trogar_Kristina_-_Sinteza_in_karakterizacija_nekaterih_halopiridinijevih_haksafluoridotitanatov.pdf Trogar_Kristina_-_Sinteza_in_karakterizacija_nekaterih_halopiridinijevih_haksafluoridotitanatov.pdf 1 12624944B4E2C0F0362185CBB753ABB1 407db80e51070e74184a611015edda08d6c88eeb36306c7e717376afe1744048 d15f4b52-5ec1-11ee-8024-0050569b8976 https://repozitorij.uni-lj.si/Dokument.php?lang=slv&id=176005 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0