20.500.12556/RUL-138925 Koordinacijske spojine cinka(II) s pikolinatom in piperidinom Coordination compounds of zinc(II) with picolinate and piperidine V diplomskem delu so opisane reakcije dveh izhodnih spojin cinka(II) s pikolinsko kislino in piperidinom. Uporabljeni izhodni spojini sta bili cinkov oksid in cinkov klorid. Reakcije so bile narejene pri sobni temperaturi, pri pogoju refluksa v acetonitrilu in segrevanju pri 105 °C v avtoklavu. Iz reakcijskih zmesi so bili izolirani trdni produkti, ki so potrdili nastanek amidina iz piperidina in acetonitrila pri opisanih reakcijskih pogojih. Izolirani trdni produkti so bili: piperidinijev klorid, pipeH[Zn(pic)3]·1,5H2O, amidinijev klorid, pipeamH[Zn(pic)3]·0,5H2O in [Zn(NH3)4]SO4·H2O. The diploma work describes reactions of two zinc(II) starting materials with picolinic acid and piperidine. Zinc oxide and zinc chloride were used as the starting materials. The reactions were carried out at ambient conditions, by heating in refluxing acetonitrile or at 105 °C in autoclaves. The isolated solids confirmed the formation of amidine from piperidine and acetonitrile under given conditions. The obtained products were: piperidinium chloride, pipeH[Zn(pic)3]·1,5H2O, amidinium chloride, pipeamH[Zn(pic)3]·0,5H2O and [Zn(NH3)4]SO4·H2O. Cink(II) pikolinat piperidin amidin koordinacijske spojine Zinc(II) picolinate piperidine amidine coordination compounds true false false Slovenski jezik Angleški jezik Diplomsko delo/naloga 2022-08-25 13:05:00 2022-08-25 13:05:02 2022-09-15 04:17:25 0000-00-00 00:00:00 2022 0 0 0000-00-00 NiDoloceno NiDoloceno NiDoloceno 0000-00-00 0000-00-00 0000-00-00 20361 120803843 Rebolj_Lara_-_Koordinacijske_spojine_cinka(II)_s_pikolinatom_in_piperidinom.pdf Rebolj_Lara_-_Koordinacijske_spojine_cinka(II)_s_pikolinatom_in_piperidinom.pdf 1 F61A5B7131BCEDE258892D77C80EB208 6994b894b15ca79e440e7c9d7e2aee2e74320172a8dd7726e3de88f9efb18016 be66f545-2465-11ed-92af-00155dcfd717 https://repozitorij.uni-lj.si/Dokument.php?lang=slv&id=159424 Fakulteta za kemijo in kemijsko tehnologijo 0 0 0